Unit 10

 

The s-block elements

 
Objectives

After studying this unit, you will be able to

describe the general charact-eristics of the alkali metals and their compounds;

explain the general characteristics of the alkaline earth metals and their compounds;

describe the manufacture, properties and uses of industrially important sodium and calcium compounds including Portland cement;

appreciate the biological significance of sodium, potassium, magnesium and calcium.

The first element of alkali and alkaline earth metals differs in many respects from the other members of the group.
 

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The s-block elements of the Periodic Table are those in which the last electron enters the outermost s-orbital. As the s-orbital can accommodate only two electrons, two groups (1 & 2) belong to the s-block of the Periodic Table. Group 1 of the Periodic Table consists of the elements: lithium, sodium, potassium, rubidium, caesium and francium. They are collectively known as the alkali metals. These are so called because they form hydroxides on reaction with water which are strongly alkaline in nature. The elements of Group 2 include beryllium, magnesium, calcium, strontium, barium and radium. These elements with the exception of beryllium are commonly known as the alkaline earth metals. These are so called because their oxides and hydroxides are alkaline in nature and these metal oxides are found in the earth’s crust*.

Among the alkali metals sodium and potassium are abundant and lithium, rubidium and caesium have much lower abundances (Table 10.1). Francium is highly radioactive; its longest-lived isotope 223Fr has a half-life of only 21 minutes. Of the alkaline earth metals calcium and magnesium rank fifth and sixth in abundance respectively in the earth’s crust. Strontium and barium have much lower abundances. Beryllium is rare and radium is the rarest of all comprising only 10–10 per cent of igneous rocks (Table 10.2, page 299).

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The general electronic configuration of s-block elements is [noble gas]ns1 for alkali metals and [noble gas] ns2 for alkaline earth metals.

* The thin, rocky outer layer of the Earth is crust. A type of rock formed from magma (molten rock) that has cooled and hardened.

Lithium and beryllium, the first elements of Group 1 and Group 2 respectively exhibit some properties which are different from those of the other members of the respective group. In these anomalous properties they resemble the second element of the following group. Thus, lithium shows similarities to magnesium and beryllium to aluminium in many of their properties. This type of diagonal similarity is commonly referred to as diagonal relationship in the periodic table. The diagonal relationship is due to the similarity in ionic sizes and /or charge/radius ratio of the elements. Monovalent sodium and potassium ions and divalent magnesium and calcium ions are found in large proportions in biological fluids. These ions perform important biological functions such as maintenance of ion balance and nerve impulse conduction.

10.1 GROUP 1 ELEMENTS: ALKALI METALS

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The alkali metals show regular trends in their physical and chemical properties with the increasing atomic number. The atomic, physical and chemical properties of alkali metals are discussed below.

 

10.1.1 Electronic Configuration

All the alkali metals have one valence electron, ns1 (Table 10.1) outside the noble gas core. The loosely held s-electron in the outermost valence shell of these elements makes them the most electropositive metals. They readily lose electron to give monovalent M+ ions. Hence they are never found in free state in nature.

table1

10.1.2 Atomic and Ionic Radii

The alkali metal atoms have the largest sizes in a particular period of the periodic table. With increase in atomic number, the atom becomes larger. The monovalent ions (M+) are smaller than the parent atom. The atomic and ionic radii of alkali metals increase on moving down the group i.e., they increase in size while going from Li to Cs.

 

10.1.3 Ionization Enthalpy

The ionization enthalpies of the alkali metals are considerably low and decrease down the group from Li to Cs. This is because the effect of increasing size outweighs the increasing nuclear charge, and the outermost electron is very well screened from the nuclear charge.

 

10.1.4 Hydration Enthalpy

The hydration enthalpies of alkali metal ions decrease with increase in ionic sizes.

Li+> Na+ > K+ > Rb+ > Cs+

Li+ has maximum degree of hydration and for this reason lithium salts are mostly hydrated, e.g., LiCl· 2H2O

 

10.1.5 Physical Properties

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All the alkali metals are silvery white, soft and light metals. Because of the large size, these elements have low density which increases down the group from Li to Cs. However, potassium is lighter than sodium. The melting and boiling points of the alkali metals are low indicating weak metallic bonding due to the presence of only a single valence electron in them. The alkali metals and their salts impart characteristic colour to an oxidizing flame. This is because the heat from the flame excites the outermost orbital electron to a higher energy level. When the excited electron comes back to the ground state, there is emission of radiation in the visible region of the spectrum as given below:

table2

Alkali metals can therefore, be detected by the respective flame tests and can be determined by flame photometry or atomic absorption spectroscopy. These elements when irradiated with light, the light energy absorbed may be sufficient to make an atom lose electron. This property makes caesium and potassium useful as electrodes in photoelectric cells.

Table 10.1 Atomic and Physical Properties of the Alkali Metals

table3

*ppm (part per million), ** percentage by weight; Lithosphere: The Earth’s outer layer: its crust and part of the upper mantle

 

10.1.6 Chemical Properties

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The alkali metals are highly reactive due to their large size and low ionization enthalpy. The reactivity of these metals increases down the group.

(i) Reactivity towards air: The alkali metals tarnish in dry air due to the formation of their oxides which in turn react with moisture to form hydroxides. They burn vigorously in oxygen forming oxides. Lithium forms monoxide, sodium forms peroxide, the other metals form superoxides. The superoxide O2 ion is stable only in the presence of large cations such as K, Rb, Cs.

(M = K, Rb, Cs)

In all these oxides the oxidation state of the alkali metal is +1. Lithium shows exceptional behaviour in reacting directly with nitrogen of air to form the nitride, Li3N as well. Because of their high reactivity towards air and water, alkali metals are normally kept in kerosene oil.

 

Problem 10.1

What is the oxidation state of K in KO2NEETprep Audio Note:  

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Solution

The superoxide species is represented as O2; since the compound is neutral, therefore, the oxidation state of potassium
is +1.

 

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  (ii) Reactivity towards water: The alkali metals react with water to form hydroxide and dihydrogen.

(M = an alkali metal)

It may be noted that although lithium has most negative E value (Table 10.1), its reaction with water is less vigorous than that of sodium which has the least negative E value among the alkali metals. This behaviour of lithium is attributed to its small size and very high hydration energy. Other metals of the group react explosively with water.

They also react with proton donors such as alcohol, gaseous ammonia and alkynes.

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  (iii) Reactivity towards dihydrogen: The alkali metals react with dihydrogen at about 673K (lithium at 1073K) to form hydrides. All the alkali metal hydrides are ionic solids with high melting points.

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  (iv) Reactivity towards halogens: The alkali metals readily react vigorously with halogens to form ionic halides, M+X. However, lithium halides are somewhat covalent. It is because of the high polarisation capability of lithium ion (The distortion of electron cloud of the anion by the cation is called polarisation). The Li+ ion is very small in size and has high tendency to distort electron cloud around the negative halide ion. Since anion with large size can be easily distorted, among halides, lithium iodide is the most covalent in nature.

(v) Reducing nature: The alkali metals are strong reducing agents, lithium being the most and sodium the least powerful
(Table 10.1). The standard electrode potential (E
) which measures the reducing power represents the overall change :

With the small size of its ion, lithium has the highest hydration enthalpy which accounts for its high negative E value and its high reducing power.

 

Problem 10.2

The E for Cl2/Cl is +1.36, for I2/I is
+ 0.53, for Ag
+ /Ag is +0.79, Na+ /Na is
–2.71 and for Li
+ /Li is 3.04. Arrange the following ionic species in decreasing order of reducing strength:

I, Ag, Cl, Li, Na  NEETprep Audio Note:  

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Solution

The order is Li > Na > I > Ag > Cl

 

(vi) Solutions in liquid ammonia: The alkali metals dissolve in liquid ammonia giving deep blue solutions which are conducting in nature.

The blue colour of the solution is due to the ammoniated electron which absorbs energy in the visible region of light and thus imparts blue colour to the solution. The solutions are paramagnetic and on standing slowly liberate hydrogen resulting in the formation of amide.

(where ‘am’ denotes solution in ammonia.)

In concentrated solution, the blue colour changes to bronze colour and becomes diamagnetic.


10.1.7 Uses

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Lithium metal is used to make useful alloys, for example with lead to make ‘white metal’ bearings for motor engines, with aluminium to make aircraft parts, and with magnesium to make armour plates. It is used in thermonuclear reactions. Lithium is also used to make electrochemical cells. Sodium is used to make a Na/Pb alloy needed to make PbEt4 and PbMe4. These organolead compounds were earlier used as anti-knock additives to petrol, but nowadays vehicles use lead-free petrol. Liquid sodium metal is used as a coolant in fast breeder nuclear reactors. Potassium has a vital role in biological systems. Potassium chloride is used as a fertilizer. Potassium hydroxide is used in the manufacture of soft soap. It is also used as an excellent absorbent of carbon dioxide. Caesium is used in devising photoelectric cells.